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Research Techniques in Organic Chemistry

出版	Prentice-Hall, 1971
主題	Science / Chemistry / Organic
ISBN	01377448979780137744893
URL	http://books.google.com.hk/books?id=wuyZRXE-Z4gC&hl=&source=gbs_api

註釋"It is a brief book on a broad topic- a practical introduction to the methods and techniques of research in organic chemistry. Synthetic techniques, analytical methods, and spectroscopic techniques- all currently most important to organic chemists- are surveyed with indications of when and how they are used. Research Techniques in Organic Chemistry is unique in that it is the only one-volume book that covers the practical aspects of major reaction, isolation, and structure determination techniques. It is practical in that the book shows the reader which methods should be applied under what conditions. It is current in that many topic important to research, yet missing in most organic chemistry books, are described, such as vacuum distillations, spinning-band distillations, sublimations, continuous extractions, high-dilution reactions, liquid ammonia reactions, vacuum line reactions, sealed tube reactions, flow pyrolyses, and the construction of constant temperature baths for kinetic studies. It is essential in that the book presents case studies of reactions in which a proposed synthesis is analyzed in detail and a synthetic method is devised to overcome inherent problems present in the synthesis. This book is useful in that there are over 60 illustrations showing many commonly used pieces of equipment. There are 16 tables covering such topics as properties of reaction solvents and recrystallization solvents, stationary phases for gas chromatography, and catalysts for hydrogenations. The introduction section includes laboratory safety precautions and instructions in use of the literature."- Publisher.